Equipment

400 MHz Bruker AVANCE III HD NMR spectrometer

• Bruker Ascend 400WB 9.4 T superconductive magnet.
• LN₂ heat exchanger system
• 4 mm ¹H – X CP MAS probe: tuning range ¹H, ³¹P-¹⁵N, temperature range -130 –150 C, 15 kHz MAS
• 10 mm ¹H – X BBO probe (liquids): tuning range ¹H, ³¹P-¹⁵N, temperature range -130 –150 C, z-gradient, ²H lock
• 5 mm ¹H –¹⁹F high temperature wideline probe: tuning range ¹H-¹⁹F, temperature range -100 – 300 C
• 5 mm X high temperature wideline probe: tuning range ¹⁰⁹Ag-³¹P, temperature range -120 – 400 C
• 5 mm X low temperature wideline probe: tuning range ¹⁴N-³¹P, Janis LHe flow cryostat, temperature range RT – 10 K

600 MHz Bruker AVANCE NEO NMR spectrometer

• Bruker Ascend 600SB  14.1 T superconductive magnet
• Bruker BCU II cooler system
• 2.5 mm ¹H – X – Y trigamma MAS probe: tuning range ¹H, ³¹P –²H, ²⁷Al – ¹⁵N, temperature range -50 –80 C, 35 kHz MAS
• 5 mm ¹H – 13C – BB TBI probe(liquids): tuning range ¹H, ¹³C, ³¹P-¹⁵N, temperature range -130 –150 C, z-gradient, 2H lock